참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Sulfur trioxide triethylamine complex | HCID 222301 | — |
| 반응물 | 3,5-Difluorobenzamide | HCID 2736910 | — |
| 용매 | Triethylamine | HCID 8471 | — |
| 생성물 | 3,5-Difluorobenzonitrile | HCID 587204 | 85.7% |
반응 단계
A suspension of 10 mmol of 3,5-difluorobenzamide and 25 mmol of triethylamine-sulphur trioxide in 30 ml of triethylamine was stirred at 89° C. for 1 hour. The working up was effected as described under Example 1a). Yield: 85.7% of theory.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05817827 |
|---|
| 출처 데이터셋 | uspto-grants-1998_10 |
|---|
| ORD ID | ord-caeff4bacf96472ca392dbc8cd0d0e74 |
|---|
| 출처 메모 | uspto-grants-1998_10 |
|---|
