반응식
[C:1]1(C(N)=O)[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][CH:2]=1.[CH2:14]([N:16](CC)CC)C.S(=O)(=O)=O>C(N(CC)CC)C>[CH:9]1[C:10]2[C:5](=[CH:4][CH:3]=[CH:2][CH:1]=2)[CH:6]=[CH:7][C:8]=1[C:14]#[N:16]참가 물질
4
반응 조건
- 온도
- 89 °C
실험 절차
A suspension of 10 mmol of naphthalenecarboxamide and 25 mmol of triethylamine-sulphur trioxide in 30 ml of triethylamine was stirred at 89° C. for 2 hours. The working up was effected as described under Example 1a). Yield: 91% of theory.
출처 및 근거
- ORD 기록
- ord-78c48b0b29fa4e708da4076fc22aa64e
- 출처 데이터셋
- uspto-grants-1998_10
- 특허 번호
- US05817827
연결된 노트
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