Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetyl chloride → 1-Methylbut-1-en-3-onyltin dibromide chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetyl chloride | HCID 6367 | — |
| 반응물 | Acetylacetone | HCID 31261 | — |
| 반응물 | Stannous bromide | HCID 66224 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | 1-Methylbut-1-en-3-onyltin dibromide chloride | HCID 85766643 | 96% |
반응 단계
The procedure was analogous to Example 6. 26.6 g (0.096 mol) of tin(II) bromide and 9.6 g (0.096 mol) of acetylacetone were reacted with 7.6 g (0.096 mol) of acetyl chloride in 200 ml of diethyl ether and the reaction solution was concentrated to give 36.4 g (96% of theory) of 1-methylbut-1-en-3-onyltin dibromide chloride (Br2 ClSn--C(CH3)=CH--CO--CH3) melting at 112°-115° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05817851 |
| 출처 데이터셋 | uspto-grants-1998_10 |
| ORD ID | ord-be6187fc3d4b4db7933cf449659e2583 |
| 출처 메모 | uspto-grants-1998_10 |