Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetyl chloride → Methyl 3-(3-bromophenyl)prop-2-enoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetyl chloride | HCID 6367 | — |
| 반응물 | 3-(3-Bromophenyl)acrylic acid | HCID 36251 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | Methyl 3-(3-bromophenyl)prop-2-enoate | HCID 610698 | — |
반응 단계
To a solution of 50.0 g (220 mmol, Aldrich) of 3-bromocinnamic acid in 1 L sieve-dried methanol (Burdick & Jackson), stirred at 0° C., was added dropwise a solution of acidic methanol (prepared by the addition of 2.5 mL acetyl chloride to 250 mL methanol). The reaction
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05827868 |
| 출처 데이터셋 | uspto-grants-1998_10 |
| ORD ID | ord-f8d184a5c3014a92bc4fb77c554723dc |
| 출처 메모 | uspto-grants-1998_10 |