Hexane → (E)-4-(Benzyloxy)-2-butenyl acetate

HRID 400232노트

반응식

HRID 400232 반응식
[C:1]([O:4][CH2:5][CH3:6])(=[O:3])[CH3:2].S(OS([O-])(=O)=O)([O-])(=O)=O.[Ce+3].S(OS([O-])(=O)=O)([O-])(=O)=O.S(OS([O-])(=O)=O)([O-])(=O)=O.[Ce+3].[CH3:36][CH2:37][CH2:38][CH2:39][CH2:40][CH3:41]>>[C:1]([O:4][CH2:5]/[CH:6]=[CH:2]/[CH2:1][O:4][CH2:5][C:38]1[CH:37]=[CH:36][CH:41]=[CH:40][CH:39]=1)(=[O:3])[CH3:2]

참가 물질

4

반응물 3

HCID 8058HexaneHCID 8857Ethyl AcetateHCID 22269528HCID 22269528, 화합물

생성물 1

HCID 14916057(E)-4-(Benzyloxy)-2-butenyl acetate

실험 절차

TLC: Rf =0.52, silica gel, 20% ethyl acetate in hexane, UV & cerium disulfate.

출처 및 근거

ORD 기록
ord-5dfb2d41abf14909bdba48dbbb2e205f
출처 데이터셋
uspto-grants-1998_10
특허 번호
US05827868

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