9-Decen-1-ol → Dec-9-enyl dec-9-enoate

HRID 400348

반응식

HRID 400348 반응식
[CH2:1]([OH:11])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH:9]=[CH2:10].[C:12](O)(=[O:22])[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH:20]=[CH2:21]>C(OCC)(=O)C.CCCCCC>[C:1]([O:22][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH:20]=[CH2:21])(=[O:11])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH:9]=[CH2:10]

참가 물질

4

반응물 2

HCID 256129-Decen-1-olHCID 617439-Decenoic acid

생성물 1

HCID 86669122Dec-9-enyl dec-9-enoate수율 92.7%

시약·촉매·용매 1

HCID 21226206Ethyl acetate hexane용매

실험 절차

Compound G was prepared from 9-decen-1-ol and 9-decenoic acid following the general procedure already discussed and shown in FIG. 12. Pure compound G was a colorless oil by column chromatography with Ethyl acetate/Hexane=1:50.

출처 및 근거

ORD 기록
ord-109817d137cf40bd88444e44967cf7a0
출처 데이터셋
uspto-grants-2014_06
특허 번호
US08741822B2

연결된 노트

불러오는 중…