Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → HCID 178497263, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Hydrazine, acetate (1:1) | HCID 165591 | — |
| 반응물 | Methyl 2,4-dioxo-4-phenylbutanoate | HCID 308117 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 생성물 | HCID 178497263 | HCID 178497263 | 66.3% |
반응 단계
983 mg hydrazine acetate was added to 2 g 2,4-Dioxo-4-phenyl-butyric acid methyl ester in 10 mL concentrated acetic acid. The mixture was stirred over night at RT. Then water was added. The precipitate was filtered, stirred with diisopropylether and again filtered to give 1.3 g desired product. Rt: 1.39 min (method O), (M+H)+: 203
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08741892B2 |
| 출처 데이터셋 | uspto-grants-2014_06 |
| ORD ID | ord-8ffbecc03032464c90cc429146c8e351 |
| 출처 메모 | uspto-grants-2014_06 |