Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methylhydrazine → HCID 178498599, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methylhydrazine | HCID 6061 | — |
| 반응물 | Dimethyl Fumarate | HCID 637568 | — |
| 생성물 | HCID 178498599 | HCID 178498599 | — |
반응 단계
Methyl hydrazine (12 ml, 228 mmol) was added dropwise to dimethyl fumarate (32.8 g, 228 mmol) at −5° C. The mixture was stirred under warming to rt for 16 h and then heated to 100° C. for 3 h. The crude reaction product (36 g, quantitative) was used for the next step without purification. [[M+H]+=159.1]
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08742106B2 |
| 출처 데이터셋 | uspto-grants-2014_06 |
| ORD ID | ord-ceefb376923e4ee2917ee93895b3fdfa |
| 출처 메모 | uspto-grants-2014_06 |