참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | Phenylhydrazine hydrochloride | HCID 60962 | — |
| 반응물 | Ethyl 2,4,5-trifluorobenzoylacetate | HCID 2758933 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | HCID 66765091 | HCID 66765091 | — |
반응 단계
Potassium carbonate (153 mg, 1.10 mmol) was added to a stirred mixture of phenyl hydrazine HCl salt (160 mg, 1.10 mmol) and ethyl 3-oxo-3-(2,4,5-trifluorophenyl)propanoate (272 mg, 1.10 mmol) in EtOH (6 mL) and the mixture was heated at 70° C. for 1 hour. The solution was cooled to room temperature and was concentrated to give the title compound, which was taken on to the next step.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US08742110B2 |
|---|
| 출처 데이터셋 | uspto-grants-2014_06 |
|---|
| ORD ID | ord-3b8aeac09dcf44bfbc8b68645c6200f3 |
|---|
| 출처 메모 | uspto-grants-2014_06 |
|---|
