Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethylacetate heptane → 6-chloro-N-methyl-4-phenylpyridazin-3-amine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethylacetate heptane | HCID 21899848 | — |
| 반응물 | 6-Chloro-4-phenylpyridazin-3-amine | HCID 76848713 | — |
| 생성물 | 6-chloro-N-methyl-4-phenylpyridazin-3-amine | HCID 86698478 | — |
반응 단계
The title compound was prepared in analogy to example 1, intermediate a, from 6-chloro-4-phenyl-pyridazin-3-ylamine and using a gradient of n-heptane:ethyl acetate (100:0 to 40:60) for the chromatographic purification. Light yellow solid (52%). MS (ESI+): m/z=220.064 ([M+H]+).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08748434B2 |
| 출처 데이터셋 | uspto-grants-2014_06 |
| ORD ID | ord-7e66c99393e84a34bdda062980d3e56e |
| 출처 메모 | uspto-grants-2014_06 |