Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Oxalate → HCID 44427818, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Oxalate | HCID 71081 | — |
| 반응물 | 1-(4-Aminobutyl)-4-(2-methoxyphenyl)piperazine | HCID 10999903 | — |
| 반응물 | 4-(2-Pyridyl)benzoic acid hydrochloride | HCID 68499643 | — |
| 생성물 | HCID 44427818 | HCID 44427818 | 53% |
반응 단계
Prepared from 4-pyridin-2-yl-benzoic acid hydrochloride and 4-(4-(2-methoxy-phenyl)-piperazin-1-yl)-butylamine according to the general procedure. Yield: 53%. Mp. (oxalate): foam. 1H NMR (CDCl3): δ1.67-1.74 (m, 4H), 2.49 (t, J 6.84, 2H), 2.67 (s, 2H), 3.07 (s, 2H), 3.51 (q, J 6.0, 2H), 3.84 (s, 3H), 6.83 (m, 5H), 7.26 (m, 1H), 7.73-7.79 (m, 2H), 7.89 (d, J 8.2, 2H), 8.06 (d, J 8.6, 2H), 8.71 (dt, J 4.7, 1.3, 1H). 13C NMR (CDCl3): δ 24.8, 27.9, 40.4, 50.8, 53.9, 55.8, 58.5, 111.6, 118.7, 121.3, 121.4, 128.1, 123.4, 127.4, 127.9, 135.6, 137.3, 142.5, 150.3, 152.7, 156.7, 167.8. Anal. (C27H32N4O2.(COOH)2.0.75H2O) C, H, N.|
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08748608B2 |
| 출처 데이터셋 | uspto-grants-2014_06 |
| ORD ID | ord-2fc03e2ec67e4cb5a945b6f861544e2b |
| 출처 메모 | uspto-grants-2014_06 |