Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzo(F)Quinoline → Mls002703342
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzo(F)Quinoline | HCID 6796 | — |
| 반응물 | Benzoyl chloride | HCID 7412 | — |
| 반응물 | Potassium Cyanide | HCID 9032 | — |
| 반응물 | Water methylene chloride | HCID 21908982 | — |
| 용매 | Water | HCID 962 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | Mls002703342 | HCID 262649 | — |
반응 단계
648 μl (5.58 mmol) benzoyl chloride was added to a two phase system of water/methylene chloride over a period of two hours. These two layers contain 500 mg (2.79 mmol) of benzo(f)chinolin in the methylene chloride layer and 545 mg (8.37 mmol) KCN in water. Stirring was continued for 6 hours. The organic phase was separated and washed with water, 5% hydrochloric acid, water, 5% NaOH solution, and again with water. After drying over magnesium sulfate, the solution was evaporated to dryness.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08753641B2 |
| 출처 데이터셋 | uspto-grants-2014_06 |
| ORD ID | ord-efdf6f83041f43f2a404661c530990f1 |
| 출처 메모 | uspto-grants-2014_06 |