Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methylamine → n-Methyl-3-nitropyridin-4-amine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methylamine | HCID 6329 | — |
| 반응물 | 4-Methoxy-3-nitropyridine | HCID 355832 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | n-Methyl-3-nitropyridin-4-amine | HCID 556016 | — |
반응 단계
2.36 g 4-methoxy-3-nitro-pyridine and 2.33 ml methylamine (40% in water) are refluxed in 25 ml of ethanol for 3 h. Then the reaction mixture is evaporated to dryness. 2.3 g product are obtained as a solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08754073B2 |
| 출처 데이터셋 | uspto-grants-2014_06 |
| ORD ID | ord-35e601a38c5e47dfb5ec3c8613cdef1f |
| 출처 메모 | uspto-grants-2014_06 |