Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(3-Benzyloxy-phenoxy)-tert-butyl-dimethyl-silane → 3-(Tert-butyldimethylsilyl)oxy-1-cyclohexanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (3-Benzyloxy-phenoxy)-tert-butyl-dimethyl-silane | HCID 58421755 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 3-(Tert-butyldimethylsilyl)oxy-1-cyclohexanol | HCID 557077 | — |
반응 단계
A mixture of 37.6 g (3-benzyloxy-phenoxy)-tert-butyl-dimethyl-silane and 3.8 g of Nishimura's catalyst in 200 ml of ethanol was hydrogenated at rt under 50 psi for 6 hours. The reaction mixture was filtered and the filtrate concentrated.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08754079B2 |
| 출처 데이터셋 | uspto-grants-2014_06 |
| ORD ID | ord-733f331f4f134e8484831a22c5f587cc |
| 출처 메모 | uspto-grants-2014_06 |