Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Methoxyphenol → 4-Methoxycyclohexanol (cis,trans)
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Methoxyphenol | HCID 9015 | — |
| 반응물 | HCID 178418361 | HCID 178418361 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 4-Methoxycyclohexanol (cis,trans) | HCID 140332 | — |
반응 단계
4-Methoxyphenol (100 g) in ethanol (759 ml) was hydrogenated under 50 psi hydrogen using Nishimura catalyst (10.0 g) at rt for 4.5 h. The catalyst was filtered off; the solvent was removed in vacuo to yield the desired product as 95% pure yellowish liquid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08754079B2 |
| 출처 데이터셋 | uspto-grants-2014_06 |
| ORD ID | ord-66c84cbcff4b405b833f38f35bbb2adf |
| 출처 메모 | uspto-grants-2014_06 |