5-Fluoro-2-nitrophenol → HCID 178454129, 화합물

HRID 406034노트

반응식

HRID 406034 반응식
[C:1]([O:5][C:6](=[O:13])[NH:7][C@H:8]1[CH2:11][C@H:10]([OH:12])[CH2:9]1)([CH3:4])([CH3:3])[CH3:2].[F:14][C:15]1[CH:16]=[CH:17][C:18]([N+:22]([O-:24])=[O:23])=[C:19](O)[CH:20]=1>>[C:1]([O:5][C:6](=[O:13])[NH:7][C@H:8]1[CH2:11][C@H:10]([O:12][C:17]2[CH:16]=[C:15]([F:14])[CH:20]=[CH:19][C:18]=2[N+:22]([O-:24])=[O:23])[CH2:9]1)([CH3:4])([CH3:2])[CH3:3]

참가 물질

3

반응물 2

HCID 99375-Fluoro-2-nitrophenolHCID 178454126HCID 178454126, 화합물

생성물 1

HCID 178454129HCID 178454129, 화합물

실험 절차

Prepared analogously to XVI.1 from 2.3 g trans-(3-Hydroxy-cyclobutyl)-carbamic acid tert-butyl ester, 1.6 g 5-fluoro-2-nitrophenol and 2.423 mIDIAD.

출처 및 근거

ORD 기록
ord-5efc6257a6674429a77da9c98ce1ac61
출처 데이터셋
uspto-grants-2014_06
특허 번호
US08754079B2

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