5-Fluoro-2-nitrophenol → HCID 58421507, 화합물

HRID 406037노트

반응식

HRID 406037 반응식
[C:1]1([OH:6])[CH2:5][CH2:4][CH2:3][CH:2]=1.[F:7][C:8]1[CH:9]=[CH:10][C:11]([N+:15]([O-:17])=[O:16])=[C:12](O)[CH:13]=1.CCOC(/N=N/C(OCC)=O)=O>>[CH:1]1([O:6][C:10]2[CH:9]=[C:8]([F:7])[CH:13]=[CH:12][C:11]=2[N+:15]([O-:17])=[O:16])[CH2:5][CH:4]=[CH:3][CH2:2]1

참가 물질

4

반응물 3

HCID 99375-Fluoro-2-nitrophenolHCID 18569CyclopentenolHCID 5462977Diethyl azodicarboxylate

생성물 1

HCID 58421507HCID 58421507, 화합물

실험 절차

Prepared analogously to XVI.1 from 1 g cyclopentenol, 1.57 g 5-fluoro-2-nitro-phenol and 1.89 ml DEAD.

출처 및 근거

ORD 기록
ord-2ec51effd80f41918983622aeb6bdc3a
출처 데이터셋
uspto-grants-2014_06
특허 번호
US08754079B2

반응 노트

불러오는 중…