4-Methoxyphenol → 4-Methoxycyclohexanol (cis,trans)

HRID 406050

반응식

HRID 406050 반응식
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([OH:9])=[CH:5][CH:4]=1.[H][H]>C(O)C>[CH3:1][O:2][CH:3]1[CH2:8][CH2:7][CH:6]([OH:9])[CH2:5][CH2:4]1

참가 물질

4

반응물 2

HCID 90154-MethoxyphenolHCID 178418361HCID 178418361, 화합물

생성물 1

HCID 1403324-Methoxycyclohexanol (cis,trans)

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

A mixture of 100 g 4-methoxyphenol and Nishimura's catalyst in 750 ml ethanol were hydrogenated (50 psi hydrogen) at room temperature for 4.5 hours. The mixture was filtered and the filtrate was concentrated.

후처리

  1. customat room temperature
  2. customfor 4.5 hours
  3. filtrationThe mixture was filtered
  4. concentrationthe filtrate was concentrated

출처 및 근거

ORD 기록
ord-eb53658046a44dc08b8875ac0fe90b71
출처 데이터셋
uspto-grants-2014_06
특허 번호
US08754079B2

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