Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → HCID 178503598, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Hydrazine hydrate (1:1) | HCID 24654 | — |
| 반응물 | 2-Benzothiazol-2-yl-3,3-bis-methylsulfanylacrylonitrile | HCID 2807727 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | HCID 178503598 | HCID 178503598 | 44% |
반응 단계
To a suspension of 2-benzothiazol-2-yl-3,3-bismethylsulfanylacrylonitrile (50 mg, 0.18 mmol) in ethanol (2 mL) was added hydrazine hydrate (15 μL). The mixture was heated to reflux for 2 hours. The reaction mixture was then cooled and water was added. The resulting precipitate was isolated by filtration to yield 21 mg (44%) of the title compound as a yellow solid. MS (m/z, ES+): 263 (M+1, 100%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08754233B2 |
| 출처 데이터셋 | uspto-grants-2014_06 |
| ORD ID | ord-dbd6832e695e455380cc1a0e31d9d7d2 |
| 출처 메모 | uspto-grants-2014_06 |