4-Iodoaniline → HCID 178462850, 화합물

HRID 40759

반응식

HRID 40759 반응식
[C:1]1(=[O:17])[N:5]([CH2:6][CH2:7][S:8](Cl)(=[O:10])=[O:9])[C:4](=[O:12])[C:3]2=[CH:13][CH:14]=[CH:15][CH:16]=[C:2]12.[I:18][C:19]1[CH:25]=[CH:24][C:22]([NH2:23])=[CH:21][CH:20]=1>>[C:4]1(=[O:12])[N:5]([CH2:6][CH3:7])[C:1](=[O:17])[C:2]2=[CH:16][CH:15]=[CH:14][CH:13]=[C:3]12.[I:18][C:19]1[CH:25]=[CH:24][C:22]([NH:23][SH:8](=[O:10])=[O:9])=[CH:21][CH:20]=1

참가 물질

3

반응물 2

HCID 108934-IodoanilineHCID 3087392-Phthalimidoethanesulfonyl chloride

생성물 1

HCID 178462850HCID 178462850, 화합물

실험 절차

Prepared according to general method A from 2-phthalimidoethanesulfonyl chloride (1.50 g) and 4-iodoaniline (2.70 g). Yield: 1.56 g (56%). 1H-NMR (CDCl3) δ (ppm) 10.14 (s, 1H), 7.83 (s, 4H), 7.63 (d, J=8.7 Hz, 2H), 7.00 (d, J=8.8 Hz, 2H), 3.94 (t, J=7.1 Hz, 2H), 3.94-3.44 (m, 2H).

후처리

  1. customPrepared

출처 및 근거

ORD 기록
ord-e1c9c55b1bcd4e9bb9e477498827aec8
출처 데이터셋
uspto-grants-2013_09
특허 번호
US08530486B2

연결된 노트

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