Toluene → 11-Bromoundecylsilane
반응식
[Br:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][Si:13](Cl)(Cl)Cl.C1(C)C=CC=CC=1>CCCCCCCCCCCCCCCC>[Br:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][SiH3:13]참가 물질
4
반응 조건
- 온도
- 60 °C
실험 절차
Freshly cleaned slides were immersed in a solution of bromoundecyl-trichlorosilane (3% v/v) in hexadecane or toluene. The reaction was heated to 60° C. for 4-6 hours then allowed to cool to room temperature. The slides were washed with CH2Cl2 and ethanol then blown dry under a stream of argon, producing a film with an advancing water contact angle of 82±2 degrees above horizontal.
후처리
- temperatureto cool to room temperature
- washThe slides were washed with CH2Cl2 and ethanol
- customthen blown dry under a stream of argon
- customproducing a film with an advancing water contact angle of 82±2 degrees above horizontal
출처 및 근거
- ORD 기록
- ord-7d1aa318407a44748ba2e762b5c1f179
- 출처 데이터셋
- uspto-grants-2014_06
- 특허 번호
- US08759008B2
반응 노트
불러오는 중…