Formic Acid → N-(2-Chloro-6-(2-chloro-6-nitrophenylthio)phenyl) formamide

반응식

[Cl:1][C:2]1[CH:8]=[CH:7][CH:6]=[C:5]([S:9][C:10]2[C:15]([N+:16]([O-:18])=[O:17])=[CH:14][CH:13]=[CH:12][C:11]=2[Cl:19])[C:3]=1[NH2:4].[CH:20](O)=[O:21]>>[Cl:1][C:2]1[CH:8]=[CH:7][CH:6]=[C:5]([S:9][C:10]2[C:15]([N+:16]([O-:18])=[O:17])=[CH:14][CH:13]=[CH:12][C:11]=2[Cl:19])[C:3]=1[NH:4][CH:20]=[O:21]

참가 물질

반응물 2

HCID 284Formic Acid

HCID 682271432-Chloro-6-(2-chloro-6-nitrophenylthio)aniline

생성물 1

HCID 86670894N-(2-Chloro-6-(2-chloro-6-nitrophenylthio)phenyl) formamide

실험 절차

A solution of 2-chloro-6-(2-chloro-6-nitrophenylthio)aniline (689 mg, 2.18 mmol) in formic acid (5 mL) was heated at reflux for 16 hours. The mixture was allowed to cool to room temperature and the solvent was evaporated. The residue was used without purification.

후처리

temperatureat reflux for 16 hours
customthe solvent was evaporated
customThe residue was used without purification

출처 및 근거

ORD 기록: ord-109483b018414b45bc19ae2b0726448b
출처 데이터셋: uspto-grants-2014_06
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08759336B2

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