Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methylamine → Methyl 4-(methylamino)-3-nitrobenzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methylamine | HCID 6329 | — |
| 반응물 | Methyl 4-chloro-3-nitrobenzoate | HCID 735797 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | Methyl 4-(methylamino)-3-nitrobenzoate | HCID 7650848 | — |
반응 단계
4-Methylamino-3-nitro-benzoic acid methyl ester (822 mg) was prepared by following General Procedure A starting from methyl 4-chloro-3-nitrobenzoate (1.0 g) and methylamine (2 M in THF, 6.95 mL) in DMF. The crude product was used in the next step without further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08759535B2 |
| 출처 데이터셋 | uspto-grants-2014_06 |
| ORD ID | ord-7f3c860dc8984f65a22b71e866d028cd |
| 출처 메모 | uspto-grants-2014_06 |