Methylamine → 2-Fluoro-4-(methylamino)-5-nitrobenzoic acid
반응식
[F:1][C:2]1[CH:10]=[C:9](F)[C:8]([N+:12]([O-:14])=[O:13])=[CH:7][C:3]=1[C:4]([OH:6])=[O:5].[CH3:15][NH2:16]>C1COCC1>[F:1][C:2]1[CH:10]=[C:9]([NH:16][CH3:15])[C:8]([N+:12]([O-:14])=[O:13])=[CH:7][C:3]=1[C:4]([OH:6])=[O:5]참가 물질
4
실험 절차
2-Fluoro-4-methylamino-5-nitro-benzoic acid (750 mg) was prepared by following General Procedure A starting from 2,4-difluoro-5-nitro-benzoic acid (1.0 g) and methylamine (2 M in THF, 2.46 mL) in THF.
출처 및 근거
- ORD 기록
- ord-23bfe7fce064480ca62974a04a9828e1
- 출처 데이터셋
- uspto-grants-2014_06
- 특허 번호
- US08759535B2
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