Sodium Methoxide → Methyl 2-methoxy-4-(methylamino)-5-nitrobenzoate
반응식
[CH3:1][O:2][C:3](=[O:16])[C:4]1[CH:9]=[C:8]([N+:10]([O-:12])=[O:11])[C:7]([NH:13][CH3:14])=[CH:6][C:5]=1F.[CH3:17][O-:18].[Na+]>CN(C=O)C>[CH3:1][O:2][C:3](=[O:16])[C:4]1[CH:9]=[C:8]([N+:10]([O-:12])=[O:11])[C:7]([NH:13][CH3:14])=[CH:6][C:5]=1[O:18][CH3:17]참가 물질
4
실험 절차
2-Methoxy-4-methylamino-5-nitro-benzoic acid methyl ester (120 mg) was prepared by following General Procedure A starting from 2-Fluoro-4-methylamino-5-nitro-benzoic acid methyl ester (200 mg) and sodium methoxide (190 mg) in DMF.
출처 및 근거
- ORD 기록
- ord-3b6cff1b10a64bd39f4a83177e8c85db
- 출처 데이터셋
- uspto-grants-2014_06
- 특허 번호
- US08759535B2
반응 노트
불러오는 중…