Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl 4-(methylamino)-3-nitrobenzoate → Methyl 3-amino-4-(methylamino)benzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl 4-(methylamino)-3-nitrobenzoate | HCID 7650848 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 생성물 | Methyl 3-amino-4-(methylamino)benzoate | HCID 15586064 | 96.1% |
반응 단계
3-amino-4-methylamino-benzoic acid methyl ester (677 mg) was prepared by following General Procedure B starting from 4-methylamino-3-nitro-benzoic acid methyl ester (822 mg) and Pd/C (10% by weight, 82 mg). The crude product was used in the next step without further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08759535B2 |
| 출처 데이터셋 | uspto-grants-2014_06 |
| ORD ID | ord-4518beb51d0246db85a61f63cb1016c4 |
| 출처 메모 | uspto-grants-2014_06 |