Sodium Azide → 1-Azido-2-(2-methoxyethoxy)ethane

HRID 410980

반응식

HRID 410980 반응식
Br[CH2:2][CH2:3][O:4][CH2:5][CH2:6][O:7][CH3:8].[N-:9]=[N+:10]=[N-:11].[Na+]>>[N:9]([CH2:2][CH2:3][O:4][CH2:5][CH2:6][O:7][CH3:8])=[N+:10]=[N-:11]

참가 물질

3

반응물 2

HCID 33557Sodium AzideHCID 1235321-Bromo-3,6-dioxaheptane

생성물 1

HCID 100347511-Azido-2-(2-methoxyethoxy)ethane수율 76.5%

실험 절차

1-Azido-2-(2-methoxy-ethoxy)-ethane (607 mg) was prepared by following General Procedure U starting from 1-bromo-2-(2-methoxy-ethoxy)-ethane (1.0 g) and sodium azide (1.07 g). The crude product was used in the next step without further purification.

후처리

  1. customThe crude product was used in the next step without further purification

출처 및 근거

ORD 기록
ord-da46aa2df9f94867b4ddaed513066231
출처 데이터셋
uspto-grants-2014_06
특허 번호
US08759535B2

연결된 노트

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