Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N-(2-Chloroethyl)dibenzylamine → [2-(2-Dibenzylamino-ethoxy)-ethyl]dimethyl-amine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N-(2-Chloroethyl)dibenzylamine | HCID 5820 | — |
| 반응물 | 2-(Dimethylamino)ethanol | HCID 7902 | — |
| 반응물 | Potassium Hydroxide | HCID 14797 | — |
| 촉매 | Tetrabutylammonium Bromide | HCID 74236 | — |
| 용매 | 1,4-Dioxane | HCID 31275 | — |
| 생성물 | [2-(2-Dibenzylamino-ethoxy)-ethyl]dimethyl-amine | HCID 67332185 | — |
반응 단계
[2-(2-Dibenzylamino-ethoxy)-ethyl]-dimethyl-amine was prepared following General Procedure S starting from dibenzyl-(2-chloro-ethyl)-amine (640 mg), 2-dimethylamino-ethanol (325 mg), 50% (w/w) KOH solution (3 mL) and tetrabutylammonium bromide (95 mg) in dioxane (3 mL).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08759535B2 |
| 출처 데이터셋 | uspto-grants-2014_06 |
| ORD ID | ord-4ae372d5b90a419eb5e8acf22be3a170 |
| 출처 메모 | uspto-grants-2014_06 |