Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N-Dimethylcarbamoylmethyl-4-methylamino-3-nitro-benzamide → 3-Amino-N-dimethylcarbamoylmethyl-4-methylamino-benzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N-Dimethylcarbamoylmethyl-4-methylamino-3-nitro-benzamide | HCID 9303598 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 3-Amino-N-dimethylcarbamoylmethyl-4-methylamino-benzamide | HCID 67333499 | 98% |
반응 단계
3-Amino-N-dimethylcarbamoylmethyl-4-methylamino-benzamide (700 mg) was prepared by following General Procedure B starting from N-dimethylcarbamoylmethyl-4-methylamino-3-nitro-benzamide (800 mg) and Pd—C (160 mg) in methanol (10 mL).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08759535B2 |
| 출처 데이터셋 | uspto-grants-2014_06 |
| ORD ID | ord-d890142553bc4e598c7639be7b6c4c30 |
| 출처 메모 | uspto-grants-2014_06 |