Iron(2+) tetrafluoroborate--water (1/2/6) → Borate(1-), tetrafluoro-, iron(2+) (2:1)

반응식

O.O.O.O.O.O.[F:7][B-:8]([F:11])([F:10])[F:9].[F:12][B-:13]([F:16])([F:15])[F:14].[Fe+2:17]>ClCCl>[F:7][B-:8]([F:11])([F:10])[F:9].[F:12][B-:13]([F:16])([F:15])[F:14].[Fe+2:17]

참가 물질

실험 절차

To a suspension of iron(II) bis(tetrafluoroborate) hexahydrate (4.9 mg; 15 μmol) in dichloromethane was added a solution of h17 (5.0 mg; 14 μmol) in a few milliliters of dichloromethane. The solution turned from light yellow to dark orange with time within 18 hours. The solution was used as is in further polymerization study.

후처리

customwithin 18 hours

출처 및 근거

ORD 기록: ord-1cf332f0753f430f9b184927c597e821
출처 데이터셋: uspto-grants-2003_05
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06559091B1

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참가 물질

반응물 1

HCID 15762351Iron(2+) tetrafluoroborate--water (1/2/6)

생성물 1

HCID 11736352Borate(1-), tetrafluoro-, iron(2+) (2:1)

시약·촉매·용매 1

HCID 6344Dichloromethane용매2회

실험 절차

후처리

customwithin 18 hours

출처 및 근거

ORD 기록: ord-1cf332f0753f430f9b184927c597e821
출처 데이터셋: uspto-grants-2003_05
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06559091B1

반응 노트

불러오는 중…