Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Phenolphthalein → Benzofurans
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Phenolphthalein | HCID 4764 | — |
| 반응물 | Epichlorohydrin | HCID 7835 | — |
| 생성물 | Benzofurans | HCID 253613 | — |
반응 단계
(A-1) 159 g of 3,3-bis(4-hydroxyphenyl)-2-benzofuran-1-on, 426.6 g of epichlorohydrin, and 160 g of a 50% alkali aqueous solution are mixed in a 1 L flask and then reacted together at 95° C. for 1 hour to form a bisphenylbenzofuran-type epoxy resin. 215 g of the bisphenylbenzofuran-type epoxy resin is mixed with 450 mg of triethylbenzylammoniumchloride, 100 mg of 2,6-diisobutylphenol, and 72 g of acrylic acid. The mixture is heated and completely dissolved at a temperature ranging from 90 to 120° C., while air is blown therein at a speed of 25 Ml per minute.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08530537B2 |
| 출처 데이터셋 | uspto-grants-2013_09 |
| ORD ID | ord-80bee22462ef451986276d8676dcb69f |
| 출처 메모 | uspto-grants-2013_09 |