Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sulfuric Acid → 5-Chlorohexanoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sulfuric Acid | HCID 1118 | — |
| 반응물 | Hexanoic Acid | HCID 8892 | — |
| 반응물 | N-Chloro-N,N-diisopropylamine | HCID 32745 | — |
| 생성물 | 5-Chlorohexanoic acid | HCID 18541668 | — |
반응 단계
155 parts by mass of the caproic acid and an equivalent amount of N-chlorodiisopropylamine were added to 1,000 parts by mass of 84% sulfuric acid and were reacted for 6 hours at 25° C. to obtain 187 parts by mass of 5-chlorocaproic acid. 187 parts by mass of the 5-chlorocaproic acid were boiled with an aqueous solution of an equivalent amount of sodium hydroxide to obtain 136 parts by mass of δ-caprolactone.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06559275B2 |
| 출처 데이터셋 | uspto-grants-2003_05 |
| ORD ID | ord-d116017f73a54474863d4eceafaa69b2 |
| 출처 메모 | uspto-grants-2003_05 |