Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methanol → methyl (2S)-4-methyl-2-(methylamino)pentanoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methanol | HCID 887 | — |
| 반응물 | 1,4-Dioxane | HCID 31275 | — |
| 반응물 | N-Methylleucine | HCID 2777993 | — |
| 용매 | Hydrochloric Acid | HCID 313 | — |
| 생성물 | methyl (2S)-4-methyl-2-(methylamino)pentanoate | HCID 10921446 | 100% |
반응 단계
N-methyl-L-leucine (1.3 g, 8.95 mmol) was dissolved in 4M HCl, 1,4-dioxane (10 mL) and methanol (10 mL). The solution was stirred overnight at room temperature, then concentrated to afford the title compound as a white solid (100%). MS (ESI): 160.0 (M+H)+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06562842B2 |
| 출처 데이터셋 | uspto-grants-2003_05 |
| ORD ID | ord-873da0f5b55f479496f9ff147aa8e0df |
| 출처 메모 | uspto-grants-2003_05 |