Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → Furan-2-acetic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Potassium Hydroxide | HCID 14797 | — |
| 반응물 | 2-Furanacetonitrile | HCID 10909515 | — |
| 생성물 | Furan-2-acetic acid | HCID 75974 | — |
반응 단계
A mixture of 2-furanacetonitrile (6.14 g), KOH (4.0 g), and water (25 mL) was refluxed for 1 hour and then cooled. Following extraction with ether, the aqueous layer was acidified to pH 2.0 with concentrated aqueous HCl. This solution was extracted with ether, and the organic phase was dried over MgSO4 and evaporated under vacuum to yield 2-furanacetic acid. The structure of the product was confirmed by NMR.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06566508B2 |
| 출처 데이터셋 | uspto-grants-2003_05 |
| ORD ID | ord-dc1b7ed696e7453f8c2cfc7d65c6a3d5 |
| 출처 메모 | uspto-grants-2003_05 |