Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,3-Dichlorobenzaldehyde → Ethyl 4-(2-chloro-6-formylphenylthio)butyrate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,3-Dichlorobenzaldehyde | HCID 35745 | — |
| 반응물 | Ethyl 4-sulfanylbutanoate | HCID 271824 | — |
| 생성물 | Ethyl 4-(2-chloro-6-formylphenylthio)butyrate | HCID 11471721 | — |
반응 단계
Ethyl 4-(2-chloro-6-formylphenylthio)butyrate was synthesized from 2,3-dichlorobenzaldehyde and ethyl 4-mercaptobutyrate in the same manner as Example 2. After column chromatography, vacuum concentration yielded ethyl 4-(2-chloro-6-formylpehylthio)butyrate (Yield 70%) as a yellow oily matter.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06566535B1 |
| 출처 데이터셋 | uspto-grants-2003_05 |
| ORD ID | ord-475a4ea6c3a14d18bc0949ac7807b9ae |
| 출처 메모 | uspto-grants-2003_05 |