Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
p-n-Octadecyloxybenzoic acid → 4-(trans-3-Decenyloxy)-benzoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | p-n-Octadecyloxybenzoic acid | HCID 139993 | — |
| 반응물 | Lithium hydroxide, monohydrate | HCID 168937 | — |
| 반응물 | Methyl-4-(trans-3-decenyloxy)-benzoate | HCID 18521096 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 4-(trans-3-Decenyloxy)-benzoic acid | HCID 18521103 | — |
반응 단계
Ester 35h (600 mg, 2.07 mmol), and lithium hydroxide monohydrate (867 mg, 20.7 mmol) in 20 ml methanol were reacted according to the procedure for compound 36a. The yield was 500 mg (87%) of a white powder which was not quite pure (95%). The product was used without further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06569504B1 |
| 출처 데이터셋 | uspto-grants-2003_05 |
| ORD ID | ord-d8c3667c163749e7a921df5f12e71ed3 |
| 출처 메모 | uspto-grants-2003_05 |