Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Bromo-2,6-dimethoxybenzoic acid → HCID 13493825, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Bromo-2,6-dimethoxybenzoic acid | HCID 2774744 | — |
| 반응물 | (1-Propylpyrrolidin-2-YL)methanamine | HCID 12829004 | — |
| 용매 | Chloroform | HCID 6212 | — |
| 생성물 | HCID 13493825 | HCID 13493825 | 79% |
반응 단계
The title compound was prepared from 3-bromo-2,6-dimethoxybenzoic acid via the acylchloride and (-)-1-n-propyl-2-(aminomethyl)pyrrolidine in the same manner as described in Example 8. Yield 79%. M.p. 103°-104° C. [α]D20 =-85.4° (c=0.5; CHCl3).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04789683 |
| 출처 데이터셋 | uspto-grants-1988_12 |
| ORD ID | ord-1248cf2a2c5c4dd19b1b4117c142eab7 |
| 출처 메모 | uspto-grants-1988_12 |