Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Iodide → HCID 21280636, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Iodide | HCID 5238 | — |
| 반응물 | N-Methylaniline | HCID 7515 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | 2-(2-(2-Chloroethoxy)ethoxy)ethanol | HCID 78871 | — |
| 용매 | 1-Butanol | HCID 263 | — |
| 생성물 | HCID 21280636 | HCID 21280636 | — |
반응 단계
A mixture of freshly distilled N-methylaniline (116 g, 1.1 mol), potassium carbonate (175 g, 1.25 mol), sodium iodide (4 g, 0.025 mol), 2-[2-(2-chloroethoxy)ethoxy]ethanol (168 g, 1 mol), and 900 mL of butanol was heated at reflux for 72 hours under nitrogen with vigorous stirring. After cooling and filtration the butanol was evaporated at reduced pressure to leave a tan oil. The oil was fractionally distilled in vacuo, yielding 150 g (63%) as a colorless oil, bp 190°-191° C. (0.13 mm).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04792208 |
| 출처 데이터셋 | uspto-grants-1988_12 |
| ORD ID | ord-d37f2b412cce47ea9333d02b28415777 |
| 출처 메모 | uspto-grants-1988_12 |