Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethanolamine → 2-(Aminomethyl)phenol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethanolamine | HCID 700 | — |
| 반응물 | Formaldehyde | HCID 712 | — |
| 반응물 | Phosphoric Acid | HCID 1004 | — |
| 반응물 | 4-tert-Butylphenol | HCID 7393 | — |
| 용매 | Water ethanol | HCID 19096565 | — |
| 생성물 | 2-(Aminomethyl)phenol | HCID 70267 | — |
반응 단계
An o-hydroxybenzylamine compound of the present invention composition was prepared according to the procedure of Example 1, except that 50 g of 4-t-butylphenol was employed in place of the Bisphenol-A, 20.1 g of ethanolamine was employed in place of the 2-(methylamino)ethanol, and that heating of the reactants was only begun after the formaldehyde addition was completed. A 0.5 g sample of the product was dissolved in 500 ml of ethanol/water (1:4 by volume) and the pH of the solution was adjusted to 3.0 with phosphoric acid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04792355 |
| 출처 데이터셋 | uspto-grants-1988_12 |
| ORD ID | ord-7486f9fc336349f2b2dc1e0a870090b4 |
| 출처 메모 | uspto-grants-1988_12 |