Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → 3-Chloroanthracen-9(10h)-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | 2-Chloroanthraquinone | HCID 8553 | — |
| 반응물 | Tin atom | HCID 5352426 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 생성물 | 3-Chloroanthracen-9(10h)-one | HCID 78601 | — |
| 생성물 | 2-Chloroanthrone | HCID 13013513 | — |
반응 단계
Tin powder (100 g) and 2-chloroanthraquinone (70 g) were refluxed in acetic acid (500 ml) while concentrated hydrochloric acid (130 ml) was added over a period of 3 hours. The solution was cooled and the product was separated by filtration, and then chromatographed on silica gel, eluting with benzene:ether, so as to afford 2-chloroanthrone and 3-chloroanthrone.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04792551 |
| 출처 데이터셋 | uspto-grants-1988_12 |
| ORD ID | ord-69046feb53fc41adb7568e4b0908623c |
| 출처 메모 | uspto-grants-1988_12 |