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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 414551생성일: 2026년 10월 26일

3-(2-Nitrophenyl)acrylic acid → Hydrocarbostyril

https://huagongshe.com/reaction/414551

반응식

참여 물질

역할이름HCID투입량
반응물3-(2-Nitrophenyl)acrylic acidHCID 92820—
촉매PalladiumHCID 23938—
용매EthanolHCID 702—
생성물HydrocarbostyrilHCID 64796—

반응 단계

A solution of 25 g of o-nitrocinnamic acid in 250 ml of ethanol was shaken with 2.5 g of 10% palladium on carbon under hydrogen at a pressure of 3 atmospheres. When the theoretical amount of hydrogen had been absorbed the catalyst was filtered off, washed with hot ethanol and the filtrate evaporated under reduced pressure to give 3,4-dihydrocarbosytril, m.p. 168°-169° C.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US04792561
출처 데이터셋uspto-grants-1988_12
ORD IDord-5ddb15b8e8ef4e80b242fcfb9689bd83
출처 메모uspto-grants-1988_12