Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-(2-Nitrophenyl)acrylic acid → Hydrocarbostyril
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-(2-Nitrophenyl)acrylic acid | HCID 92820 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | Hydrocarbostyril | HCID 64796 | — |
반응 단계
A solution of 25 g of o-nitrocinnamic acid in 250 ml of ethanol was shaken with 2.5 g of 10% palladium on carbon under hydrogen at a pressure of 3 atmospheres. When the theoretical amount of hydrogen had been absorbed the catalyst was filtered off, washed with hot ethanol and the filtrate evaporated under reduced pressure to give 3,4-dihydrocarbosytril, m.p. 168°-169° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04792561 |
| 출처 데이터셋 | uspto-grants-1988_12 |
| ORD ID | ord-5ddb15b8e8ef4e80b242fcfb9689bd83 |
| 출처 메모 | uspto-grants-1988_12 |