Calcium Carbonate → HCID 178419798, 화합물

HRID 414628

반응식

HRID 414628 반응식
[S:1].[CH2:2]1[CH:6]2[C@@H:7]3[CH:11]=[CH:10][C@H:9]([CH:5]2[CH:4]=[CH:3]1)[CH2:8]3.C(=O)([O-])[O-].[Ca+2]>O>[S:1].[CH2:2]1[CH:6]2[C@@H:7]3[CH:11]=[CH:10][C@H:9]([CH:5]2[CH:4]=[CH:3]1)[CH2:8]3

참가 물질

5

반응물 3

HCID 10112Calcium CarbonateHCID 5362487SulfurHCID 15618652endo-Dicyclopentadiene

생성물 1

HCID 178419798HCID 178419798, 화합물

시약·촉매·용매 1

HCID 962Water용매

실험 절차

Into a 4 liter autoclave were placed 425 g of sulfur, 75 g of DCPD, 2500 ml of water, 20 g of calcium carbonate and 5.0 g of Igepal®-630 (GAF). The reactor was sealed and heated to 150° for three hours with stirring. After cooling to room temperature, the sulfur/DCPD adduct was isolated as small ribbons.

후처리

  1. customThe reactor was sealed
  2. temperatureheated to 150° for three hours

출처 및 근거

ORD 기록
ord-511ec55e90004ba1bae3a0571b85130c
출처 데이터셋
uspto-grants-1988_12
특허 번호
US04792589

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