Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Nitric Acid → 4-Methyl-6-nitro-7-hydroxy-1-indanone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Nitric Acid | HCID 944 | — |
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 반응물 | 7-Hydroxy-4-methyl-1-indanone | HCID 12436244 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 생성물 | 4-Methyl-6-nitro-7-hydroxy-1-indanone | HCID 13604142 | — |
반응 단계
Into a solution of 25.6 g of 4-methyl-7-hydroxy-1-indanone in 250 ml of acetic acid was added 19.4 ml of acetic anhydride and a solution of 15.4 ml of concentrated nitric acid in 50 ml of acetic acid gradually. The reaction mixture was concentrated to drynsss, and the residue was washed with ether to obtain 25.7 g of 4-methyl-6-nitro-7-hydroxy-1-indanone.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04792628 |
| 출처 데이터셋 | uspto-grants-1988_12 |
| ORD ID | ord-5cb9e452ae114983b72b93924d0f9940 |
| 출처 메모 | uspto-grants-1988_12 |