Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sulfuric Acid → 4-Methyl-6-aminomethyl-7-hydroxy-1-indanone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sulfuric Acid | HCID 1118 | — |
| 반응물 | 4-Methyl-6-alpha-chloroacetylaminomethyl-7-hydroxy-1-indanone | HCID 13604141 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 4-Methyl-6-aminomethyl-7-hydroxy-1-indanone | HCID 13604144 | — |
반응 단계
3 Grams of 4-methyl-6-α-chloroacetylaminomethyl-7-hydroxy-1-indanone and a solution of 30 ml of concentrated sulfuric acid in 60 ml of ethanol were refluxed by heating for 8 hours. The solvent was removed by evaporation, the residue thus obtained was recrystallized from ethanol to obtain 1 g of 4-methyl-6-aminomethyl-7-hydroxy-1-indanone.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04792628 |
| 출처 데이터셋 | uspto-grants-1988_12 |
| ORD ID | ord-d178894b4e4c4482b7509e98b99d4b09 |
| 출처 메모 | uspto-grants-1988_12 |