Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dichloromethane → 4-Methyl-6-allyl-7-hydroxy-1-indanone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dichloromethane | HCID 6344 | — |
| 반응물 | Hexane | HCID 8058 | — |
| 반응물 | 4-Methyl-7-allyloxy-1-indanone | HCID 13604147 | — |
| 용매 | Tetralin | HCID 8404 | — |
| 생성물 | 4-Methyl-6-allyl-7-hydroxy-1-indanone | HCID 13604148 | — |
반응 단계
32 Grams of 4-methyl-7-allyloxy-1-indanone was suspended in 100 ml of tetrahydronaphthalene. The suspension was refluxed by heating for 4 hours under argon gas atmosphere. The reaction mixture was subjected to a silica gel column chromatography (eluent: n-hexane, and dichloromethane: n-hexane=1:2) to obtain 26.8 g of 4-methyl-6-allyl-7-hydroxy-1-indanone.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04792628 |
| 출처 데이터셋 | uspto-grants-1988_12 |
| ORD ID | ord-ea059138b91c421798de0321bae6ec3f |
| 출처 메모 | uspto-grants-1988_12 |