Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrogen Bromide → HCID 68820841, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrogen Bromide | HCID 260 | — |
| 반응물 | Dimethyl Sulfoxide | HCID 679 | — |
| 반응물 | methyl N-[3-(6,7-dimethoxy-2-methylaminoquinazolin-4-yl)phenyl]terephthalamic acid | HCID 66646296 | — |
| 용매 | Isopropanol | HCID 3776 | — |
| 생성물 | HCID 68820841 | HCID 68820841 | — |
반응 단계
Dimethyl sulfoxide (1 mL) and hydrobromic acid (40 μL) were added to methyl N-[3-(6,7-dimethoxy-2-methylaminoquinazolin-4-yl)phenyl]terephthalamic acid (100.90 mg). 2-Propanol (5 mL) was added to the mixture while heating the mixture, and the mixture was cooled to room temperature to be solidified. The solid was collected by filtration to yield the titled compound (108.92 mg).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08530654B2 |
| 출처 데이터셋 | uspto-grants-2013_09 |
| ORD ID | ord-c3aa049b7aa9465693f6054ed6d6261f |
| 출처 메모 | uspto-grants-2013_09 |