2-Methylfuran → HCID 58288601, 화합물

HRID 41665

반응식

HRID 41665 반응식
[C:1]1(=[O:7])[CH:5]=[CH:4][C:3](=[O:6])[CH2:2]1.[CH3:8][C:9]1[O:10][CH:11]=[CH:12][CH:13]=1>CO>[CH3:8][C:9]12[O:10][CH:11]([CH:12]=[CH:13]1)[CH:4]1[CH:5]2[C:1](=[O:7])[CH2:2][C:3]1=[O:6]

참가 물질

4

반응물 2

HCID 107972-MethylfuranHCID 702582-Cyclopentene-1,4-dione

생성물 1

HCID 58288601HCID 58288601, 화합물

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

A mixture of 4-cyclopentene-1,3-dione (10 g, 104 mmol) and 2-methylfuran (15 ml) are stirred at room temperature for 3 days. Methanol (50 ml) is then added and the solid is collected and dried on a Buchner funnel to give 1-methyl-10-oxa-tricyclo[5.2.1.0*2,6*]dec-8-ene-3,5-dione (14.3 g)

후처리

  1. customthe solid is collected
  2. customdried on a Buchner funnel

출처 및 근거

ORD 기록
ord-31f574acb1d14478b81e748c79a80f90
출처 데이터셋
uspto-grants-2013_09
특허 번호
US08530667B2

연결된 노트

불러오는 중…