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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 4169생성일: 2026년 10월 23일

N-methylpropyn-2-ylamine → 5,11-Dihydro-11-[[N-methyl(2-propynyl)amino]carbonyl]-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one

https://huagongshe.com/ko/reaction/4169

반응식

참여 물질

역할이름HCID투입량
반응물N-methylpropyn-2-ylamineHCID 96160—
반응물11-chlorocarbonyl-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-oneHCID 11043962—
생성물5,11-Dihydro-11-[[N-methyl(2-propynyl)amino]carbonyl]-6H-pyrido[2,3-b][1,4]benzodiazepin-6-oneHCID 20152918—

반응 단계

Analogously to Example C, using 27.3 g (0.1 mol) of 11-chlorocarbonyl-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one and 7.0 g (0.1 mol) of N-methyl-propargylamine, 27 g (88% of theory) of the desired compound are obtained.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US04724236
출처 데이터셋uspto-grants-1988_02
ORD IDord-40ce053f6f454522aede5b77a4a32553
출처 메모uspto-grants-1988_02