참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Chloroform | HCID 6212 | — |
| 반응물 | Hexafluoropropylene | HCID 8302 | — |
| 생성물 | CCl3CF2CHFCF3 | HCID 12829385 | — |
반응 단계
A 0.5 inch (12.7 mm) by 40 inch (101.6 cm) plug flow reactor that is packed with Helipack Monel support is heated to 290° C. A 50/50 (molar %) mixture of hexafluoropropene and chloroform is fed into the reactor at about 1.5 g/min. The reactor pressure is maintained at 100 psig. The effluent from the reactor is fed into a distillation column and the unreacted reagents removed by distillation and recycled. The product CCl3CF2CHFCF3 is used in the next reaction.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US08530709B2 |
|---|
| 출처 데이터셋 | uspto-grants-2013_09 |
|---|
| ORD ID | ord-e25e851eb2fd41f9bfbe6fa77cb92408 |
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| 출처 메모 | uspto-grants-2013_09 |
|---|
