Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Monoethyl malonate → HCID 178516622, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Monoethyl malonate | HCID 70615 | — |
| 반응물 | Sodium t-butoxide | HCID 23676156 | — |
| 반응물 | 1-Isocyano-2-methylpropan-2-yl methyl carbonate | HCID 25267464 | — |
| 반응물 | 4-(4,4-Difluoropiperidin-1-yl)benzaldehyde | HCID 86670877 | — |
| 반응물 | HCID 178507353 | HCID 178507353 | — |
| 생성물 | HCID 178516622 | HCID 178516622 | — |
반응 단계
The compound was synthesized starting from 1H-benzo[d]imidazol-5-amine (0.890 g, 6.69 mmol), 4-(4,4-difluoropiperidin-1-yl)benzaldehyde (1.5 g, 6.69 mmol), 2-(ethoxycarbonyl)acetic acid (0.883 g, 6.69 mmol), 1-isocyano-2-methylpropan-2-yl methyl carbonate (1.05 g, 6.69 mmol) and sodium tert.-butoxide (0.713 g, 6.35 mmol) according to method 3.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08530670B2 |
| 출처 데이터셋 | uspto-grants-2013_09 |
| ORD ID | ord-04d66ba45c82473a8f4ab8194da2842e |
| 출처 메모 | uspto-grants-2013_09 |